1-(3-氯苯氧基)-2-羟丁-3-炔合成路线 （共 4 条）
反应条件
in tetrahydrofuran
T=0 - 20°C; 16 h;
参考文献
Fox, Martin E.; Jackson, Mark; Lennon, Ian C.; McCague, Raymond; Parratt, Julian S.
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 50 - 56
参考文献
Fox, Martin Edward; Parratt, Julian Simon
Patent: US2001/9770 A1, 2001 ;
反应条件
1: 73 percent / K2CO3 / 1-methyl-pyrrolidin-2-one / 140 - 150 °C
2: 90 percent / aq. H2SO4 / tetrahydrofuran / 20 h / Heating
3: 85 percent / tetrahydrofuran / 16 h / 0 - 20 °C
View Scheme
参考文献
Fox, Martin E.; Jackson, Mark; Lennon, Ian C.; McCague, Raymond; Parratt, Julian S.
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 50 - 56
反应条件
1: 90 percent / aq. H2SO4 / tetrahydrofuran / 20 h / Heating
2: 85 percent / tetrahydrofuran / 16 h / 0 - 20 °C
View Scheme
参考文献
Fox, Martin E.; Jackson, Mark; Lennon, Ian C.; McCague, Raymond; Parratt, Julian S.
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 1 p. 50 - 56
