7-氯-3-甲基-1H-吲哚合成路线 （共 9 条）
反应条件
(CH3)S*BH3 in tetrahydrofuran
24 h; Ambient temperatureTHF*BH3;
参考文献
Wierenga, Wendell; Griffin, John; Warpehoski, Martha A.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2437 - 2440
反应条件
(CH3)S*BH3 in tetrahydrofuran
24 h; Ambient temperatureTHF*BH3;
参考文献
Wierenga, Wendell; Griffin, John; Warpehoski, Martha A.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2437 - 2440
反应条件
dimethylsulfide borane complex in tetrahydrofuran
24 h; Ambient temperatureTHF*BH3;
参考文献
Wierenga, Wendell; Griffin, John; Warpehoski, Martha A.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2437 - 2440
反应条件
in tetrahydrofuran
T=-40°C; 1 h;
参考文献
Didier, Charles; Critcher, Douglas J.; Walshe, Nigel D.; Kojima, Yasuhiro; Yamauchi, Yuji; Barrett, Anthony G. M.
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7875 - 7879
反应条件
1: tetrahydrofuran / 0 °C
2: 90 percent / (CH3)S*BH3 / tetrahydrofuran / 24 h / Ambient temperature; THF*BH3
View Scheme
参考文献
Wierenga, Wendell; Griffin, John; Warpehoski, Martha A.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2437 - 2440
反应条件
2: 82 percent / (CH3)2S*BH3 / tetrahydrofuran / 24 h / Ambient temperature; THF*BH3
View Scheme
参考文献
Wierenga, Wendell; Griffin, John; Warpehoski, Martha A.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2437 - 2440
反应条件
in tetrahydrofuran
T=-40°C; 1 h; Further byproducts given;
参考文献
Bosco, Marcella; Dalpozzo, Renato; Bartoli, Giuseppe; Palmieri, Gianni; Petrini, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 5 p. 657 - 663
反应条件
in tetrahydrofuran
T=0°C;
参考文献
Bosco, Marcella; Dalpozzo, Renato; Bartoli, Giuseppe; Palmieri, Gianni; Petrini, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 5 p. 657 - 663
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
12 h;
参考文献
Didier, Charles; Critcher, Douglas J.; Walshe, Nigel D.; Kojima, Yasuhiro; Yamauchi, Yuji; Barrett, Anthony G. M.
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7875 - 7879
