苄基2-(2-萘基氨基甲酰)-1-吡咯烷羧酸酯合成路线 (共 4 条)
反应条件
1: dicyclohexylcarbodiimide / tetrahydrofuran / 3 h / 0 °C
2: tetrahydrofuran / 1.) 3 h, 0 deg C; 2.) 12 h, r.t.
View Scheme
参考文献
Hauzer, Karel; Servitova, Linda; Barth, Tomislav; Jost, Karel
Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 4 p. 1139 - 1148
反应条件
in tetrahydrofuran
1.) 3 h, 0 deg C; 2.) 12 h, r.t.; Yield given;
参考文献
Hauzer, Karel; Servitova, Linda; Barth, Tomislav; Jost, Karel
Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 4 p. 1139 - 1148
反应条件
chloroform; triethylamine; toluene
anschliessend Erwaermen mit <2>Naphthylamin;
参考文献
Folk; Burstone
Archives of Biochemistry, 1956 , vol. 61, p. 257,258
反应条件
1: HBr / acetic acid / 0.17 h / Ambient temperature
2: N-ethylpiperidine / dimethylformamide / 12 h / Ambient temperature
View Scheme
参考文献
Hauzer, Karel; Servitova, Linda; Barth, Tomislav; Jost, Karel
Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 4 p. 1139 - 1148