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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
869355-04-4
合成路线
（共 9 条）
4637-24-5
N,N-二甲基甲酰胺二甲基缩醛
+
3608-58-0
3’-脱氧鸟苷
→
反应条件
869355-04-4
反应条件
in methanol
参考文献
Bhan, Purshotam; Bhan, Anila; Hong, Mikung; Hartwell, John G.; Saunders, June M.; Hoke, GlennD
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1195 - 1199
17331-16-7
→
反应条件
869355-04-4
反应条件
1: 90 percent 2: 83 percent / H2O / acetonitrile / 0 °C 3: 91 percent / tri-n-butyltin hydride; 2,2'-azobisisoburtyronitrile / toluene / 2 h / 95 °C 4: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0 °C 5: 100 percent / aq. ammonia / methanol View Scheme
参考文献
Cui, Zhiyong; Zhang, Lei; Zhang, Biliang
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 561 - 563
118-00-3
鸟苷
→
反应条件
869355-04-4
反应条件
1: 97 percent / acetonitrile 2: 90 percent 3: 83 percent / H2O / acetonitrile / 0 °C 4: 91 percent / tri-n-butyltin hydride; 2,2'-azobisisoburtyronitrile / toluene / 2 h / 95 °C 5: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0 °C 6: 100 percent / aq. ammonia / methanol View Scheme
参考文献
Cui, Zhiyong; Zhang, Lei; Zhang, Biliang
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 561 - 563
160905-87-3
→
反应条件
869355-04-4
反应条件
1: 83 percent / H2O / acetonitrile / 0 °C 2: 91 percent / tri-n-butyltin hydride; 2,2'-azobisisoburtyronitrile / toluene / 2 h / 95 °C 3: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0 °C 4: 100 percent / aq. ammonia / methanol View Scheme
参考文献
Cui, Zhiyong; Zhang, Lei; Zhang, Biliang
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 561 - 563
329014-12-2
→
反应条件
869355-04-4
反应条件
1: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0 °C 2: 100 percent / aq. ammonia / methanol View Scheme
参考文献
Cui, Zhiyong; Zhang, Lei; Zhang, Biliang
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 561 - 563
247223-54-7
→
反应条件
869355-04-4
反应条件
1: 91 percent / tri-n-butyltin hydride; 2,2'-azobisisoburtyronitrile / toluene / 2 h / 95 °C 2: 100 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0 °C 3: 100 percent / aq. ammonia / methanol View Scheme
参考文献
Cui, Zhiyong; Zhang, Lei; Zhang, Biliang
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 561 - 563
34097-37-5
N,N-1H-嘌呤-2,6-二双乙酰胺
→
反应条件
869355-04-4
反应条件
1: 1.) BSA, TMSOTf / 1.) DCE, 2.) TolH 2: 87 percent / NH4OH / methanol / 48 h / 60 °C 3: 100 percent / adenosine deaminase, phosphate buffer / dimethylsulfoxide; H2O 4: 92 percent / methanol View Scheme
参考文献
Bhan, Purshotam; Bhan, Anila; Hong, Mikung; Hartwell, John G.; Saunders, June M.; Hoke, GlennD
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1195 - 1199
3608-57-9
→
反应条件
869355-04-4
反应条件
1: 100 percent / adenosine deaminase, phosphate buffer / dimethylsulfoxide; H2O 2: 92 percent / methanol View Scheme
参考文献
Bhan, Purshotam; Bhan, Anila; Hong, Mikung; Hartwell, John G.; Saunders, June M.; Hoke, GlennD
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1195 - 1199
112233-74-6
N,N-二苯基-氨基甲酸 2-(乙酰氨基)-9H-嘌呤-6-基酯
→
反应条件
869355-04-4
反应条件
1: 1.) BSA, TMSOTf / 1.) DCE, 2.) TolH 2: 87 percent / NH4OH / methanol / 48 h / 60 °C 3: 92 percent / methanol View Scheme
参考文献
Bhan, Purshotam; Bhan, Anila; Hong, Mikung; Hartwell, John G.; Saunders, June M.; Hoke, GlennD
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1195 - 1199
