3-(3-氯苯基)-5-异恶唑甲醛合成路线 (共 6 条)
反应条件
silica gel; pyridinium chlorochromate in dichloromethane T=20°C;
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 7 p. 2449 - 2452
反应条件
1.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 20 - 60 °C / Inert atmosphere 1.2: 50 °C / Inert atmosphere 2.1: silica gel; pyridinium chlorochromate / dichloromethane / 20 °C View Scheme
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 7 p. 2449 - 2452
反应条件
1.1: pyridine / 20 °C 2.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 20 - 60 °C / Inert atmosphere 2.2: 50 °C / Inert atmosphere 3.1: silica gel; pyridinium chlorochromate / dichloromethane / 20 °C View Scheme
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 7 p. 2449 - 2452
反应条件
silica gel; pyridinium chlorochromate in dichloromethane
T=20°C;
参考文献
Landge, Kamalkishor P.; Oh, Ji Seon; Pae, Ae Nim; Park, Woo Kyu; Gong, Jae Yang; Koh, Hun Yeong; Jung, Sun Ho
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 7 p. 2449 - 2452
反应条件
1.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 20 - 60 °C / Inert atmosphere
1.2: 50 °C / Inert atmosphere
2.1: silica gel; pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Landge, Kamalkishor P.; Oh, Ji Seon; Pae, Ae Nim; Park, Woo Kyu; Gong, Jae Yang; Koh, Hun Yeong; Jung, Sun Ho
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 7 p. 2449 - 2452
反应条件
1.1: pyridine / 20 °C
2.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 20 - 60 °C / Inert atmosphere
2.2: 50 °C / Inert atmosphere
3.1: silica gel; pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Landge, Kamalkishor P.; Oh, Ji Seon; Pae, Ae Nim; Park, Woo Kyu; Gong, Jae Yang; Koh, Hun Yeong; Jung, Sun Ho
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 7 p. 2449 - 2452