water in hexane
in sealed evacuated ampule; to a soln. of Et3GeLi at -78°C CF3CONEt2 added; stirred at - 78°C for 3; hydrolized; dried; CF3COGeEt3 isolated by fractionation; PMR; GLC; mass-spectrometry; elem. anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 1654 - 1658
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 1838 - 1843
