[(5-溴-2,3-二氢-1H-茚-1-基)氧基](1,1-二甲基乙基)二甲基硅烷合成路线 （共 3 条）
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in DMF (N,N-dimethyl-formamide)
T=20°C; 3 h;
参考文献
Xue, Chu-Biao; Cao, Ganfeng; Huang, Taisheng; Chen, Lihua; Zhang, Ke; Wang, Anlai; Meloni, David; Anand, Rajan; Glenn, Joseph; Metcalf, Brian W.
Patent: US2005/261310 A1, 2005 ;
Location in patent: Page/Page column 35 ;
US 20050261310 A1
反应条件
in dichloromethane
T=0°C; 0.5 h;
参考文献
LG LIFE SCIENCES, LTD.
Patent: WO2009/38411 A2, 2009 ;
Location in patent: Page/Page column 39 ;
WO 2009/038411 A2
反应条件
1: 2-bromo-1,3-thiazole With chloro-trimethyl-silane; ethylene dibromide; zinc in tetrahydrofuran
0.25 h;
2: [(5-bromo-2,3-dihydro-1H-inden-1-yl)oxy](tert-butyl)dimethylsilane With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
24 h; Heating / reflux;
参考文献
Xue, Chu-Biao; Cao, Ganfeng; Huang, Taisheng; Chen, Lihua; Zhang, Ke; Wang, Anlai; Meloni, David; Anand, Rajan; Glenn, Joseph; Metcalf, Brian W.
Patent: US2005/261310 A1, 2005 ;
Location in patent: Page/Page column 35 ;
US 20050261310 A1
