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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
86984-22-7
合成路线
（共 8 条）
10467-10-4
乙基镁碘
+
26032-72-4
2,4-二氯-6-(4-苯基)-嘧啶
→
反应条件
86984-22-7
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether T=0°C;
参考文献
Elmoghayar, Mohamed R. H.; Groth, Per; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 2 p. 109 - 114
89967-19-1
→
反应条件
86984-22-7
反应条件
trichlorophosphate 3 h; Heating;
参考文献
Sakamoto, Takao; Sakasai, Takeji; Yoshizawa, Hiroshi; Tanji, Ken-Ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4554 - 4560
86984-18-1
→
反应条件
86984-22-7
反应条件
1: 20 percent / triethylamine / toluene / 5 h / Heating 2: 55 percent / dichloro-1,3-bis(diphenylphosphinopropane)nickel(II) / diethyl ether / 0 °C View Scheme
参考文献
Elmoghayar, Mohamed R. H.; Groth, Per; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 2 p. 109 - 114
86984-17-0
→
反应条件
86984-22-7
反应条件
1: 84 percent / triethylamine / toluene / 5 h / Heating 2: 55 percent / dichloro-1,3-bis(diphenylphosphinopropane)nickel(II) / diethyl ether / 0 °C View Scheme
参考文献
Elmoghayar, Mohamed R. H.; Groth, Per; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 2 p. 109 - 114
5331-64-6
→
反应条件
86984-22-7
反应条件
1: 70 percent / conc. HCl / ethanol / 48 h / Heating 2: 85 percent / phosphoryl chloride / 3 h / Heating View Scheme
参考文献
Sakamoto, Takao; Sakasai, Takeji; Yoshizawa, Hiroshi; Tanji, Ken-Ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4554 - 4560
86984-22-7
→
反应条件
74502-97-9
反应条件
ammonium hydroxide; hydrogen; palladium on activated charcoal in methanol
参考文献
Sakamoto, Takao; Sakasai, Takeji; Yoshizawa, Hiroshi; Tanji, Ken-Ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4554 - 4560
86984-22-7
→
反应条件
89967-11-3
反应条件
1: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol 2: 79 percent / propyl nitrite, HCl / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Sakamoto, Takao; Sakasai, Takeji; Yoshizawa, Hiroshi; Tanji, Ken-Ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4554 - 4560
86984-22-7
→
反应条件
64571-51-3
反应条件
1: 96 percent / hydrogen/conc. ammonia / 5percent palladium charcoal / methanol 2: 79 percent / propyl nitrite, HCl / ethanol / 2 h / Ambient temperature 3: 81 percent / pyruvic acid, conc. HCl / aq. ethanol / 6 h / Heating View Scheme
参考文献
Sakamoto, Takao; Sakasai, Takeji; Yoshizawa, Hiroshi; Tanji, Ken-Ichi; Nishimura, Sumiko; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4554 - 4560
