5-(4-甲酰基苯基)噻吩-2-甲醛合成路线 (共 3 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether
T=80°C; Suzuki cross-coupling; 30 h;
参考文献
Costa, Susana P. G.; Batista, Rosa M. F.; Cardoso, Paulo; Belsley, Michael; Raposo, Maria Manuela M.
European Journal of Organic Chemistry, 2006 , # 17 p. 3938 - 3946
反应条件
sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in water; N,N-dimethyl-formamide
Suzuki coupling reaction;
参考文献
Kuhnert, Nikolai; Patel, Chirag; Jami, Fatemeh
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7575 - 7579
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide
T=150°C; Heck reaction; 20 h; Inert atmosphere;
参考文献
Roger, Julien; Pozgan, Franc; Doucet, Henri
Green Chemistry, 2009 , vol. 11, # 3 p. 425 - 432