乙氧基甲叉丙二酸二乙酯合成路线 (共 444 条)
反应条件
ethanol; nickel T=100 - 125°C; Hydrogenation;
参考文献
Hogberg; Vora; Drake; et al.
1984 , vol. 38, # 5 B p. 359 - 366
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate T=0 - 20°C; 2 h; Title compound not separated from byproducts;
参考文献
Reding, Matthew T.; Kaburagi, Yosuke; Tokuyama, Hidetoshi; Fukuyama, Tohru
Heterocycles, 2002 , vol. 56, # 1-2 p. 313 - 330
反应条件
T=125°C; Hydrogenation;
参考文献
Adkins; Billica
Journal of the American Chemical Society, 1948 , vol. 70, p. 3121
反应条件
1: ethanol / 2 h / |Reflux 2: diphenylether / 1 h / |Reflux View Scheme
参考文献
Podanyi, Benjamin; Kereszturi, Geza; Vasvari-Debreczy, Lelle; Chinoin, Istvan Hermecz; Toth, Gabor
Magnetic Resonance in Chemistry, 1996 , vol. 34, # 11 p. 972 - 978
反应条件
1: 130 °C View Scheme
参考文献
De; Byers; Krogstad
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 1 p. 315 - 320
反应条件
potassium hydroxide in methanol 0.0833333 h; Ambient temperature;
参考文献
Alaiz, Manuel; Giron, Julio; Hidalgo, Francisco Javier; Maza, Maria Pilar de la; Millan, Francisco; et al.
Synthesis, 1989 , # 7 p. 544 - 547
反应条件
in diethyl ether 1.) 0 deg C, 0.25 h; 2.) 23 deg C, 0.5 h.;
参考文献
Clemo, Nicholas G.; Pattenden, Gerald
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2133 - 2136
反应条件
1: allyl bromide With indium in tetrahydrofuran T=20°C; 1 h; 2: aniline; diethyl 2-ethoxymethylenemalonate in tetrahydrofuran 2 h;
参考文献
Organic Letters, , vol. 8, # 2 p. 195 - 198
反应条件
in ethanol T=28°C; 0.333333 h;
参考文献
Chemistry - A European Journal, , vol. 16, # 9 p. 2938 - 2943
反应条件
1: ethanol / 5 h / Heating 2: H2 / Raney-Ni / ethanol / Ambient temperature 3: diethyl ether / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 104, p. 715 - 729