1: 3-fluoro-phenol With sodium hydride in N,N-dimethyl-formamide 2: 3-oxo-1,3-dihydro-isobenzofuran in N,N-dimethyl-formamide T=160°C; 5 h; Product distribution / selectivity;
1: diethylamine With AlCl3, aluminium chloride in 1,2-dichloro-ethane
T=20 - 25°C; 0.416667 h;
2: 3-oxo-1,3-dihydro-isobenzofuran in 1,2-dichloro-ethane
0.75 h;
3: With water in 1,2-dichloro-ethane
T=0°C; 0.5 h;