反应条件
1: 1,1,2,3,4,4-hexachloro-1,3-butadiene With n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; 2.75 h; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=0 - 20°C; 1.75 h; Inert atmosphere;
参考文献
Drew, Samuel L.; Lawrence, Andrew L.; Sherburn, Michael S.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4221 - 4224
Angew. Chem., 2013 , vol. 125, # 15 p. 4315 - 4318,4