L-(+)-酒石酸二乙酯合成路线 (共 47 条)
参考文献
Bucher
American Chemical Journal, 1900 , vol. 23, p. 75
参考文献
D'Ianni; Adkins
Journal of the American Chemical Society, 1939 , vol. 61, p. 1675,1676
反应条件
1: NaIO4 on SiO2 / dichloromethane / 20 °C
2: cerium(III) chloride heptahydrate; sodium tetrahydroborate / ethanol / 20 °C
View Scheme
参考文献
Janthawornpong, Karnjapan; Krasutsky, Sergiy; Chaignon, Philippe; Rohmer, Michel; Poulter, C. Dale; Seemann, Myriam
Journal of the American Chemical Society, 2013 , vol. 135, # 5 p. 1816 - 1822
反应条件
4 A molecular sieve; toluene-4-sulfonic acid in toluene
72 h; Heating;
参考文献
Wuensch, Bernhard; Nerdinger, Sven
European Journal of Organic Chemistry, 1998 , # 4 p. 711 - 718
反应条件
in various solvent(s)
T=170°C; 175 h;
参考文献
Shainyan; Ustinov; Bel'skii; Nindakova
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 1 p. 104 - 110
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; MeOAMVN in acetic acid
T=55°C; 3 h; light-shielding conditions; Product distribution / selectivity;
参考文献
Daiichi Sankyo Company, Limited
Patent: EP2298763 A1, 2011 ;
Location in patent: Page/Page column 26 ;
EP 2298763 A1
反应条件
T=70°C; Ausbildung eines Gleichgewichts mit ca. 45percent Fufural-(Z)-oxim (es erfolgt partielle Umwandlung);
参考文献
Patterson et al.
Journal of the Chemical Society, 1941 , p. 606