3,5-二叔丁基-4-羟基苄基甲基醚合成路线 （共 47 条）
反应条件
potassium hydroxide; iodine in methanol
other bases, other solvent; Product distribution;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3046 - 3050
反应条件
sodium methylate in methanol
Ambient temperatureelectrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.1 M NaClO4; 0.5 V; effect of the electricity consumption; Product distributionMechanism;
参考文献
Ohmori, Hidenobu; Ueda, Chihiro; Tokuno, Yoshimi; Maeda, Hatsuo; Masui, Masaichiro
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 9 p. 4007 - 4011
反应条件
rate constant of the disproportionation; Rate constantThermodynamic data;
参考文献
Roginskii, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 1833 - 1841
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 9 p. 1987 - 1996
反应条件
1: potassium hydroxide / methanol / 3 h / 65 °C
2: 97 percent / sodium borohydride / ethanol / Heating
View Scheme
参考文献
Kerr, David I. B.; Khalafy, Jabbar; Ong, Jennifer; Perkins, Michael V.; Prager, Rolf H.; Puspawati, Ni Made; Rimaz, Mehdi
Australian Journal of Chemistry, 2006 , vol. 59, # 7 p. 457 - 462
反应条件
potassium hydroxide; acetic acid in methanol; nitromethane; nitrogen
参考文献
FMC Corporation
Patent: US4024186 A1, 1977 ;
反应条件
sulfuric acid in acetic acid
T=20 - 60°C; 6 h; Inert atmosphere;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
potassium hydroxide in methanol
T=65°C; 3 h;
参考文献
The Goodyear Tire and Rubber Company
Patent: US4284823 A1, 1981 ;
