1-溴-3-甲基-2-丁烯合成路线 (共 689 条)
反应条件
phosphorus tribromide T=0°C; 30 h;
参考文献
Chow, Siew Yin; Williams, Howard J.; Huang, Qiulong; Nanda, Samik; Scott, A. Ian
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 9997 - 10003
反应条件
pyridine; phosphorus tribromide; sodium chloride in water
参考文献
Rolfe, James; Allen, Warrick
Patent: US2009/156706 A1, 2009 ;
反应条件
silica gel; phosphorus tribromide in dichloromethane T=-10°C; 0.416667 h;
参考文献
De Mattos, Marcio C. S.; Sanseverino, Antonio Manzolillo
Synthetic Communications, 2003 , vol. 33, # 13 p. 2181 - 2186
反应条件
hydrogen bromide T=0°C; 0.5 h;
参考文献
Vani; Chida; Srinivasan; Chandrasekharam; Singh
Synthetic Communications, 2001 , vol. 31, # 2 p. 219 - 224
反应条件
in dichloromethane T=20°C; 1 h;
参考文献
Kishali, Nurhan; Polat, M. Fatih; Altundas, Ramazan; Kara, Yunus
Helvetica Chimica Acta, 2008 , vol. 91, # 1 p. 67 - 72
反应条件
1: 91 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C 2: 83 percent / HBr / CH2Cl2 / 1.5 h / 0 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 23 p. 4654 - 4663
反应条件
sodium acetate in water; acetic acid 3 h;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 37, # 9 p. 803 - 808
反应条件
1: LiAlH4 / diethyl ether 2: 48percent HBr, conc. H2SO4 View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 60, p. 1169 - 1171
反应条件
1: lithium alanate; diethyl ether 2: pyridine; petroleum ether; phosphorus (III)-bromide View Scheme
参考文献
Helvetica Chimica Acta, , vol. 34, p. 186,189
反应条件
2: hydrogen bromide / dann Umsetzung des erhaltenen 2-Brom-2-methyl-butens-(3) View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 105, p. 72
Chemische Berichte, , vol. 58, p. 279 Anm. 15