1-溴-3-甲基-2-丁烯合成路线 (共 689 条)
反应条件
allyl zinc bromide in tetrahydrofuran T=65°C; MechanismProduct distribution;
参考文献
Godschalx, J. P.; Stille, J. K.
Tetrahedron Letters, 1983 , vol. 24, # 18 p. 1905 - 1908
参考文献
Godschalx, J. P.; Stille, J. K.
Tetrahedron Letters, 1983 , vol. 24, # 18 p. 1905 - 1908
反应条件
hydrogenchloride; anhydrous guanidine 1) EtOH, 1 h; Yield given. Multistep reaction;
参考文献
Crombie, Leslie; Jarrett, Sandra R. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 23 p. 3179 - 3184
反应条件
sodium hydride; sodium iodide in ethylene glycol dimethyl ether T=20°C; 5 h;
参考文献
Trost, Barry M.; Toste, F. Dean
Journal of the American Chemical Society, 2002 , vol. 124, # 18 p. 5025 - 5036
反应条件
1: With NiI2; iodine; sodium iodide; iron; triethylamine in dichloromethane; acetone T=20°C; atmospheric pressure; 2: With hydrogenchloride; air in dichloromethane; acetone
参考文献
Nadal, M. Lluisa; Bosch, Julia; Vila, Josep M.; Klein, Guenter; Ricart, Susagna; Moreto, Josep M.
Journal of the American Chemical Society, 2005 , vol. 127, # 30 p. 10476 - 10477
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2998,3000; engl. Ausg. S. 3339, 3341
反应条件
potassium carbonate in acetone T=60°C; 16 h;
参考文献
Pu, Jun; Deng, Kangwen; Butera, John; Chlenov, Michael; Gilbert, Adam; Kagan, Mike; Mattes, James; Resnick, Lynn
Tetrahedron, 2010 , vol. 66, # 11 p. 1963 - 1972
参考文献
Pochini,A. et al.
Gazzetta Chimica Italiana, 1975 , vol. 105, p. 1253 - 1258
反应条件
1: sodium methylate; methanol; diethyl ether 2: palladium; acetic acid / Hydrogenation View Scheme
参考文献
Riedl
Chemische Berichte, 1952 , vol. 85, p. 692,704, 708
反应条件
1: NaBH4 / ethanol / 2 h / 15 - 20 °C 2: H2O2 / 2 h / 15 - 20 °C / var. oxidants and time. View Scheme
参考文献
Tetrahedron Letters, , vol. 26, # 7 p. 921 - 924