1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
chloroform und Wasserdampfdestillation in Stickstoffatmosphaere;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2913
反应条件
lithium hydride in dimethyl sulfoxide 45 deg C, 5 h; 25 deg C, 10 h;
参考文献
Tetrahedron Letters, , vol. 39, # 45 p. 8221 - 8224
反应条件
lead(II) bromide; aluminium in acetonitrile 15 h;
参考文献
Khanna, R.N.; Singh, Prem Kumar
Synthetic Communications, 1990 , vol. 20, # 12 p. 1743 - 1749
反应条件
diethyl ether T=0°C;
参考文献
Fieser
Journal of the American Chemical Society, 1927 , vol. 49, p. 857
Journal of the American Chemical Society, 1928 , vol. 50, p. 447
反应条件
1: 300 mg / zinc dust / tetrahydrofuran / 4 h 2: 30 mg / 1percent aq.NaOH / 0.42 h / Heating View Scheme
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 189 - 191
参考文献
Cooke
Australian Journal of Scientific Research, Series A: Physical Sciences, 1950 , vol. 3, p. 481,484,485
参考文献
Fieser
Journal of the American Chemical Society, 1926 , vol. 48, p. 3202,3206
Journal of the American Chemical Society, 1927 , vol. 49, p. 858,861
反应条件
1: 14 percent / K2CO3 / methanol / 10 h / Ambient temperature 2: 82 percent / Dowex 50 / methanol / 24 h / 40 °C View Scheme
参考文献
Fukai, Toshio; Nomura, Taro
Heterocycles, 1992 , vol. 34, # 6 p. 1213 - 1225
反应条件
chloro-trimethyl-silane; tetrakis(dimethylamino)ethylene; Chromium (III) chloride; niobium bromide in N,N-dimethyl-formamide T=20°C; Acylation; Reduction; 6 h;
参考文献
Synlett, , # 12 p. 1930 - 1932
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.25 h / -70 °C 1.2: 82 percent / tetrahydrofuran / -70 - 20 °C 2.1: 70 percent / diethyl ether / 1 h / 0 °C View Scheme
参考文献
Gebhard, R.; Courtin, J. M. L.; Shadid, J. B.; Haveren, J. van; Haeringen, C. J. van; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1989 , vol. 108, # 6 p. 207 - 214
