1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
n-butyllithium; potassium tert-butylate; diisopropylamine 1.) THF/hexane, -70 deg C, 5 min 2.) THF/hexane; Yield given. Multistep reaction;
参考文献
Klusener, P. A. A.; Tip, L.; Brandsma, L.
Tetrahedron, 1991 , vol. 47, # 10/11 p. 2041 - 2064
反应条件
bis(1,5-cyclooctadiene)nickel (0) 1.) benzene, 0 deg C, 20 min, 2.) DMF, 0 deg C, 2 h; r.t., 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gazzetta Chimica Italiana, , vol. 114, # 9/10 p. 443 - 450
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
1: EtMgBr / tetrahydrofuran / 0 °C 2: H2 / Pd-C / methanol View Scheme
参考文献
Yadav; Valluri; Rama Rao
Tetrahedron Letters, 1994 , vol. 35, # 21 p. 3609 - 3612
反应条件
tetra-n-propylammonium bromide in dichloromethane 24 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , # 4 p. 630 - 636
反应条件
copper(I) bromide in dichloromethane T=20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 39, # 19 p. 3111 - 3126
反应条件
2: 1.) NaH / 1.) THF, 15 min, room temperature, 2.) 1.5 h, room temperature 3: 1.) NaH / 1.) THF; 2.) 20 h, -78 deg C 4: 1.) CuI / 1.) THF, 10 min, -78 deg C; 2.) 2 h, -78 deg C View Scheme
参考文献
Mori, Kenji; Fujiwhara, Mitsuhiko
Liebigs Annalen der Chemie, 1989 , p. 41 - 44
