1-溴-3-甲基-2-丁烯合成路线 (共 689 条)
反应条件
indium(III) chloride; water; zinc in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Araki, Shuki; Jin, Shun-Ji; Idou, Yoshiyuki; Butsugan, Yasuo
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 6 p. 1736 - 1738
反应条件
zinc in tetrahydrofuran T=55 - 60°C; 4 h;
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 189 - 191
反应条件
zinc in tetrahydrofuran 4 h; Further byproducts given;
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 189 - 191
反应条件
in acetonitrile 2 h; Ambient temperature;
参考文献
Davisson, V. Jo; Woodside, Andrew B.; Neal, Timothy R.; Stremler, Kay E.; Muehlbacher, Manfred; Poulter, C. Dale
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 4768 - 4779
反应条件
tris(tetra-n-butylammonium)hydrogen diphosphate in acetonitrile 24 h; Ambient temperature; Yield given;
参考文献
Dixit, Vyas M.; Laskovics, F. Mark; Noall, Wendy I.; Poulter, C. Dale
Journal of Organic Chemistry, 1981 , vol. 46, # 9 p. 1967 - 1969
反应条件
potassium carbonate in toluene T=90°C; 3 h; regioselective reaction;
参考文献
Scrivanti, Alberto; Beghetto, Valentina; Bertoldini, Matteo; Matteoli, Ugo
European Journal of Organic Chemistry, 2012 , # 2 p. 264 - 268
反应条件
1: thiophenol With sodium hydride in ethanol T=20°C; 1 h; Inert atmosphere; 2: prenyl bromide in ethanol T=20°C; Inert atmosphere;
参考文献
Holzwarth, Michael S.; Alt, Isabel; Plietker, Bernd
Angewandte Chemie - International Edition, 2012 , vol. 51, # 22 p. 5351 - 5354
反应条件
sodium methylate in methanol T=0 - 20°C; 1 h;
参考文献
Greenman, Kevin L; Carter, David S; Van Vranken, David L
Tetrahedron, 2001 , vol. 57, # 24 p. 5219 - 5225
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane 24 h; Heating;
参考文献
Majumdar; Khan; Chattopadhyay
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 5 p. 483 - 485
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C;
参考文献
Garro Hugo; Manzur Jimena; Ciuffo Gladys; Tonn Carlos; Pungitore Carlos
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 3 p. 760 - 764