1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
1.1: LDA / tetrahydrofuran; hexane / 1 h / -78 °C 1.2: 87 percent / tetrahydrofuran; hexane / -78 - 20 °C 2.1: 94 percent / LiAlH4 / tetrahydrofuran / 4 h / 0 °C 3.1: 79 percent / DMSO; oxalyl chloride; Et3N / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Trost, Barry M.; Toste, F. Dean
Journal of the American Chemical Society, 2002 , vol. 124, # 18 p. 5025 - 5036
参考文献
Armesto, Diego; Austin, Mark A.; Griffiths, Owain J.; Horspool, William M.; Carpintero, Mercedes
Chemical Communications, 1996 , # 24 p. 2715 - 2716
反应条件
(i) EtMgBr, (ii) /BRN= 1420778/; Multistep reaction;
参考文献
Dillenberger,Z. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 1856 - 1902
反应条件
(i) EtMgBr, THF, (ii) /BRN= 1420778/, THF; Multistep reaction;
参考文献
Julia,S. et al.
Bulletin de la Societe Chimique de France, 1966 , p. 3499 - 3507
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
ytterbium in tetrahydrofuran T=20°C; 9 h;
参考文献
Gohain, Mukut; Gogoi, Baikuntha J.; Prajapati, Dipak; Sandhu, Jagir S.
New Journal of Chemistry, 2003 , vol. 27, # 7 p. 1038 - 1040
反应条件
Zn/Gr 5 h; Ambient temperature;
参考文献
Marceau, P.; Gautreau, L.; Beguin, F.; Guillaumet, G.
Journal of Organometallic Chemistry, 1991 , vol. 403, # 1.2 p. 21 - 27
