1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
参考文献
Johnson,C.R. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 13 p. 2065 - 2067
反应条件
sodium hydride
1.) THF, 0.5 h, 2.) overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brownbridge, Peter; Hunt, Paul G.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1695 - 1706
反应条件
indium; triphenylphosphine; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in N,N-dimethyl-formamide
T=100°C; 25 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
反应条件
indium; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=100°C; 1 h;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in toluene
T=110°C; Suzuki-Miyaura coupling; 17 h; Inert atmosphere;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; indium; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide
T=100°C; 20 h; Inert atmosphere;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
反应条件
palladium diacetate in 1,4-dioxane
T=100°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
1: 28 percent / NaH / toluene / 24 h / 35 °C
2: 73 percent / aluminium chloride; HCl / cyclohexane / 2.5 h / 20 °C
View Scheme
参考文献
Hurd; Hoffman
Journal of Organic Chemistry, 1940 , vol. 5, p. 212,218
反应条件
Montmorillonite K10 clay in tetrachloromethane
2 h;
参考文献
Dintzner, Matthew R.; McClelland, Kristen M.; Morse, Kara M.; Akroush, Michael H.
Synlett, 2004 , # 11 p. 2028 - 2030
反应条件
Montmorillonite K10 clay in tetrachloromethane
2 h;
参考文献
Dintzner, Matthew R.; McClelland, Kristen M.; Morse, Kara M.; Akroush, Michael H.
Synlett, 2004 , # 11 p. 2028 - 2030
