1-溴-3-甲基-2-丁烯合成路线 (共 689 条)
反应条件
Montmorillonite K10 clay in tetrachloromethane
2 h;
参考文献
Dintzner, Matthew R.; McClelland, Kristen M.; Morse, Kara M.; Akroush, Michael H.
Synlett, 2004 , # 11 p. 2028 - 2030
反应条件
potassium hydroxide in water
T=0°C;
参考文献
Crombie; Jones; Palmer
Tetrahedron Letters, 1985 , vol. 26, # 24 p. 2929 - 2932
反应条件
water; palladium diacetate; potassium carbonate in toluene
T=90°C; 3 h;
参考文献
Scrivanti, Alberto; Beghetto, Valentina; Bertoldini, Matteo; Matteoli, Ugo
European Journal of Organic Chemistry, 2012 , # 2 p. 264 - 268
反应条件
water; palladium diacetate; potassium carbonate in toluene
T=90°C; 3 h;
参考文献
Scrivanti, Alberto; Beghetto, Valentina; Bertoldini, Matteo; Matteoli, Ugo
European Journal of Organic Chemistry, 2012 , # 2 p. 264 - 268
反应条件
copper(l) iodide; boron trifluoride diethyl etherate in diethyl ether
other Lewis acids, solvents; Product distribution;
参考文献
Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
反应条件
zinc in tetrahydrofuran
24 h; Further byproducts given;
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 189 - 191
参考文献
Birch, Arthur J.; Kelly, Lawrence F.; Narula, Acharan S.
Tetrahedron, 1982 , vol. 38, # 12 p. 1813 - 1824
反应条件
magnesium
Multistep reaction;
参考文献
Hamana, Hiroshi; Sugasawa, Tsutomu
Chemistry Letters, 1985 , p. 921 - 924
反应条件
1: ethyl 3,3-dimethyl-acrylate With lithium diisopropyl amide in tetrahydrofuran; n-heptane
T=-78°C; 0.25 h; Inert atmosphere;
2: prenyl bromide in tetrahydrofuran; n-heptane
T=-78°C; 1 h; Inert atmosphere;
参考文献
Pepper, Henry P.; Tulip, Stephen J.; Nakano, Yuji; George, Jonathan H.
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2564 - 2573
反应条件
chloro-trimethyl-silane in dichloromethane
P=7500600 Torr; 48 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Yamamoto, Yoshinori; Hatsuya, Satoshi; Yamada, Jun-ichi
Journal of the Chemical Society, Chemical Communications, 1988 , # 24 p. 1639 - 1640