1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
magnesium in diethyl ether
参考文献
Hua, Duy H.; Miao, Shou Wu; Chen, Jin Shan; Iguchi, Sadahiko
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 4 - 6
反应条件
(i) PhLi, THF, (ii) Li, MeNH2; Multistep reaction;
参考文献
Bhalerao,U.T.; Rapoport,H.
Journal of the American Chemical Society, 1971 , vol. 93, p. 5311 - 5313
反应条件
copper(l) iodide; magnesium
1.) THF, 35-40 deg C, 15 min, 2.) room temp., overnight; Yield given. Multistep reaction;
参考文献
Parr, William J. E.
Journal of Chemical Research, Miniprint, 1981 , # 11 p. 4101 - 4130
反应条件
bis(1,5-cyclooctadiene)nickel (0)
1.) benzene, 0 deg C, 20 min, 2.) DMF, 0 deg C, 2 h; r.t., 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carpita, Adriano; Bonaccorsi, Fabrizio; Rossi, Renzo
Gazzetta Chimica Italiana, 1984 , vol. 114, # 9/10 p. 443 - 450
反应条件
in diethyl ether; hexane
3 h; Ambient temperature;
参考文献
Araki, Shuki; Jin, Shun-Ji; Butsugan, Yasuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 5 p. 549 - 552
反应条件
copper(l) iodide; boron trifluoride diethyl etherate in diethyl ether
other Lewis acids, solvents; Product distribution;
参考文献
Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 398,401;engl.Ausg.S.421,423
参考文献
Nilsson, Ylva I.M.; Andersson, Pher G.; Baeckvall, Jan-E.
Journal of the American Chemical Society, 1993 , vol. 115, # 15 p. 6609 - 6613
反应条件
aluminium trichloride; iron in water
T=20°C; 5 h;
参考文献
Saikia, Promod; Laskar, Dhrubojyoti D.; Prajapati, Dipak; Sandhu, Jagir S.
Chemistry Letters, 2001 , # 6 p. 512 - 513
反应条件
1: 1) n-BuLi / THF, hexane
2: 68 percent / Raney Ni / acetone; ethanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Weyerstahl, Peter; Schenk, Anja; Marschall, Helga
Liebigs Annalen, 1995 , # 10 p. 1849 - 1854
