1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
diethyl ether; magnesium
参考文献
Staudinger; Kreis; Schilt
Helvetica Chimica Acta, 1922 , vol. 5, p. 750
反应条件
lithium aluminium tetrahydride; silver perchlorate in tetrahydrofuran T=-20°C; 0.5 h;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Chemistry Letters, 1983 , p. 1877 - 1878
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; potassium tert-butylate 1.) hexane, -15 deg C, 0.3 h; 2.) -15-20 deg C, 12h; time, temperature; Product distributionMechanism;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, Christian
Journal of Organometallic Chemistry, 1988 , vol. 344, p. 9 - 28
反应条件
methanol; diethyl ether; sodium methylate
参考文献
Spaeth; Holzen
Chemische Berichte, 1935 , vol. 68, p. 1123,1125
反应条件
potassium carbonate in acetone 1 h; Heating;
参考文献
Row; Brown; Stachulski; Lennard
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 8 p. 1604 - 1610
反应条件
1: 40 percent / lithium hydride / dimethylsulfoxide / 45 deg C, 5 h; 25 deg C, 10 h 2: H2SO4 / H2O / 25 °C View Scheme
参考文献
Schaffner-Sabba, Karl; Schmidt-Ruppin, Karl H.; Wehrli, Walter; Schuerch, ALfred R.; Wasley, Jan W. F.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 8 p. 990 - 994
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yanagisawa, Akira; Noritake, Yoshiyuki; Yamamoto, Hisashi
Chemistry Letters, 1988 , p. 1899 - 1902
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.25 h / -70 °C 1.2: 82 percent / tetrahydrofuran / -70 - 20 °C 2.1: 70 percent / diethyl ether / 1 h / 0 °C 3.1: NaH / tetrahydrofuran / 0 - 20 °C 3.2: 89.4 percent / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Jansen, Frans Jos H. M.; Lugtenburg, Johan
European Journal of Organic Chemistry, 2000 , # 5 p. 829 - 836
反应条件
zinc(II) chloride; benzene
参考文献
Livingstone; Whiting
Journal of the Chemical Society, 1955 , p. 3631,3635
反应条件
potassium carbonate; potassium iodide in acetone T=80°C; 12 h;
参考文献
Cheng, Chia-Fu; Lai, Zhen-Chang; Lee, Yean-Jang
Tetrahedron, 2008 , vol. 64, # 19 p. 4347 - 4353
