1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
potassium carbonate in acetone
Heating;
参考文献
Tatsuzaki, Jin; Bastow, Kenneth F.; Nakagawa-Goto, Kyoko; Nakamura, Seiko; Itokawa, Hideji; Lee, Kuo-Hsiung
Journal of Natural Products, 2006 , vol. 69, # 10 p. 1445 - 1449
反应条件
potassium carbonate; sodium iodide in acetone
Heating;
参考文献
Majumdar; Kundu
Synthetic Communications, 2006 , vol. 36, # 21 p. 3191 - 3201
反应条件
Yield given. Multistep reaction;
参考文献
Masson, S.; Mothes, V.; Thuillier, A.
Tetrahedron, 1984 , vol. 40, # 9 p. 1573 - 1580
反应条件
Yield given. Multistep reaction;
参考文献
Masson, S.; Mothes, V.; Thuillier, A.
Tetrahedron, 1984 , vol. 40, # 9 p. 1573 - 1580
反应条件
1.1: LiHMDS / tetrahydrofuran / 1 h / 20 °C
2.1: DIBAL-H / diethyl ether; hexane / -70 - 20 °C
3.1: 84 percent / K2CO3 / methanol / 3.5 h
4.1: n-butyllithium / hexane; tetrahydrofuran / 1.5 h / -78 °C
4.2: 92 percent / hexane; tetrahydrofuran / -78 - 20 °C
View Scheme
参考文献
Boyer, Francois-Didier; Hanna, Issam
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5181 - 5188
反应条件
lithium hexamethyldisilazane in tetrahydrofuran
T=20°C; 1 h;
参考文献
Boyer, Francois-Didier; Hanna, Issam
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5181 - 5188
反应条件
1: LiHMDS / tetrahydrofuran / 1 h / 20 °C
2: DIBAL-H / diethyl ether; hexane / -70 - 20 °C
View Scheme
参考文献
Boyer, Francois-Didier; Hanna, Issam
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5181 - 5188
反应条件
1: LiHMDS / tetrahydrofuran / 1 h / 20 °C
2: DIBAL-H / diethyl ether; hexane / -70 - 20 °C
3: 84 percent / K2CO3 / methanol / 3.5 h
View Scheme
参考文献
Boyer, Francois-Didier; Hanna, Issam
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5181 - 5188
反应条件
zinc in tetrahydrofuran
T=20°C; Barbier reaction; 4.5 h;
参考文献
Yadav; Reddy; Reddy, P.Muralikrishna; Srinivas
Tetrahedron Letters, 2002 , vol. 43, # 29 p. 5185 - 5187
反应条件
zinc in tetrahydrofuran
T=20°C; Barbier reaction; 4.5 h;
参考文献
Yadav; Reddy; Reddy, P.Muralikrishna; Srinivas
Tetrahedron Letters, 2002 , vol. 43, # 29 p. 5185 - 5187
