1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
1.1: tert.-butyl lithium / tetrahydrofuran; n-heptane / 0.08 h / -78 °C / |Inert atmosphere
1.2: 4.08 h / -50 °C / |Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Schmidt, Jens; Stark, Christian B. W.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 1920 - 1928
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Tyrrell, Elizabeth; Tesfa, Kibur Hunie; Millet, Julien; Muller, Christophe
Synthesis, 2006 , # 18 p. 3099 - 3105
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Mann, Alastair; Muller, Christophe; Tyrrell, Elizabeth
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 8 p. 1427 - 1438
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Tyrrell, Elizabeth; Tesfa, Kibur Hunie; Millet, Julien; Muller, Christophe
Synthesis, 2006 , # 18 p. 3099 - 3105
反应条件
copper(II) bis(trifluoromethanesulfonate)
T=100°C; 16 h; regioselective reaction;
参考文献
Zhang, Yugen; Chen, Liwei; Lu, Ting
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 7 p. 1055 - 1060
反应条件
Yield given. Multistep reaction;
参考文献
Corey, E. J.; Dittami, James P.
Journal of the American Chemical Society, 1985 , vol. 107, p. 256 - 257
反应条件
sodium hydride in tetrahydrofuran
T=25°C;
参考文献
Nakahira, Hiroyuki; Sunagawa, Makoto
Tetrahedron Letters, 1997 , vol. 38, # 25 p. 4443 - 4446
参考文献
Karrer et al.
Helvetica Chimica Acta, 1939 , vol. 22, p. 1287,1290
反应条件
potassium carbonate in acetone
Heating;
参考文献
Watanabe; Kawada; Hirata; Maki; Imada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3551 - 3560
反应条件
lead(II) bromide; aluminium in acetonitrile
8 h;
参考文献
Khanna, R.N.; Singh, Prem Kumar
Synthetic Communications, 1990 , vol. 20, # 12 p. 1743 - 1749
