1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
10percent NaOH
T=20°C; 5 h;
参考文献
Uto, Yoshihiro; Hirata, Akihiko; Fujita, Tomoya; Takubo, Syunsuke; Nagasawa, Hideko; Hori, Hitoshi
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2355 - 2357
反应条件
1: 2 h / Ambient temperature
2: 87 percent / NaOH / tetrahydrofuran / 5 h / Ambient temperature
View Scheme
参考文献
Xu; Lu; Huang
Synthetic Communications, 1993 , vol. 23, # 18 p. 2527 - 2531
参考文献
Pochini,A. et al.
Gazzetta Chimica Italiana, 1975 , vol. 105, p. 1253 - 1258
反应条件
potassium carbonate in ethylene glycol dimethyl ether
7 h; Heating; Further byproducts given;
参考文献
Rodighiero, Paolo; Guiotto, Adriano; Pastorini, Giovanni; Manzini, Paolo; Dall'Acqua, Francesco; et al.
Gazzetta Chimica Italiana, 1980 , vol. 110, # 2/3 p. 167 - 172
反应条件
potassium carbonate in ethylene glycol dimethyl ether
7 h; Heating; Further byproducts given;
参考文献
Rodighiero, Paolo; Guiotto, Adriano; Pastorini, Giovanni; Manzini, Paolo; Dall'Acqua, Francesco; et al.
Gazzetta Chimica Italiana, 1980 , vol. 110, # 2/3 p. 167 - 172
反应条件
potassium carbonate in acetone
14 h; Ambient temperature;
参考文献
Ito; Fujiwara; Kajita; Ju-ichi; Takemura; Suzuki; Tanaka; Omura; Furukawa
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 10 p. 2509 - 2513
反应条件
sodium acetate; acetic acid
参考文献
Bigi, Franca; Casiraghi, Giovanni; Casnati, Giuseppe; Sartori, Giovanni
Synthesis, 1981 , # 4 p. 310 - 312
反应条件
1: 85 percent / Na / diethyl ether / 48 h / 36 °C
2: (Ce(NH4)2(NO3)6) / acetonitrile; H2O / 0 °C
3: Na2S2O4 / acetone / 25 °C
View Scheme
参考文献
Bouzbouz, Samir; Kirschleger, Bernard; Villieras, Jean
Bulletin de la Societe Chimique de France, 1997 , vol. 134, # 1 p. 67 - 84
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=55°C; P=1551.4 Torr; 36 h;
参考文献
Yang; Wong
Tetrahedron, 1994 , vol. 50, # 32 p. 9583 - 9608
反应条件
chloro-trimethyl-silane; zinc in N,N-dimethyl-formamide
T=20°C; Barbier-type reaction; 1 h;
参考文献
Legros, Julien; Meyer, Franck; Coliboeuf, Matthieu; Crousse, Benoit; Bonnet-Delpon, Daniele; Begue, Jean-Pierre
Journal of Organic Chemistry, 2003 , vol. 68, # 16 p. 6444 - 6446
