1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
参考文献
Baird,M.S. et al.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 210 - 211
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene
T=50°C; 4 h; Further byproducts given;
参考文献
Reisch; Mueller; Mester
1981 , vol. 36, # 9 p. 1176 - 1179
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene
T=50°C; 4 h; Product distribution;
参考文献
Reisch; Mueller; Mester
1981 , vol. 36, # 9 p. 1176 - 1179
反应条件
1.1: KOH; Bu4NBr / CH2Cl2; acetonitrile / 0.25 h
1.2: 97 percent / CH2Cl2; acetonitrile / 2 h
2.1: 61 percent / aq. NH3 / ethanol / 7 h / 20 °C
3.1: MeSO3H / dioxane
View Scheme
参考文献
Carmignani; Volpe; Botta; Espinal; De Bonnevaux; De Luca; Corelli; Tafi; Sacco; Delle Monache
Journal of Medicinal Chemistry, 2001 , vol. 44, # 18 p. 2950 - 2958
反应条件
in ethanol; water
1 h; Ambient temperature;
参考文献
Hebrard,P.; Olomucki,M.
Bulletin de la Societe Chimique de France, 1970 , p. 1938 - 1942
反应条件
Yield given. Multistep reaction;
参考文献
Masson, S.; Mothes, V.; Thuillier, A.
Tetrahedron, 1984 , vol. 40, # 9 p. 1573 - 1580
反应条件
Yield given. Multistep reaction;
参考文献
Masson, S.; Mothes, V.; Thuillier, A.
Tetrahedron, 1984 , vol. 40, # 9 p. 1573 - 1580
反应条件
potassium carbonate in chloroform
18 h; Ambient temperature;
参考文献
Miller,J.A. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 603 - 606
反应条件
in N,N-dimethyl-formamide
参考文献
Silverbrook Research Pty Ltd; Indusegaram, Sutharsiny; Gonzaga, Graciel; Vonwiller, Simone Charlotte; Starling, Scott Matthew; Hall, Lachlan Everett; Ridley, Damon Donald; Silverbrook, Kia
Patent: US2014/94601 A1, 2014 ;
Location in patent: Page/Page column ;
反应条件
sodium iodide in acetone
T=0°C; 0.166667 h;
参考文献
Celebuski, J.; Rosenblum, M.
Tetrahedron, 1985 , vol. 41, # 24 p. 5741 - 5746
