1-溴-3-甲基-2-丁烯合成路线 （共 689 条）
参考文献
Claisen
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 72
Chemische Berichte, 1925 , vol. 58, p. 279 Anm. 15
参考文献
Claisen
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 72
Chemische Berichte, 1925 , vol. 58, p. 279 Anm. 15
反应条件
1: KH, 18-crown-6 / diethyl ether; paraffin / 24 h / Heating 2: KOH, H2O / methanol / 3 h / 25 °C View Scheme
参考文献
Doyle, Michael P.; Kalinin, Alexey V.
Journal of Organic Chemistry, 1996 , vol. 61, # 6 p. 2179 - 2184
反应条件
potassium carbonate in acetone 4 h;
参考文献
Reed, Michael W.; Moore, Harold W.
Journal of Organic Chemistry, 1988 , vol. 53, # 8 p. 4166 - 4171
反应条件
1: 1.) KOH / 1.) DMSO, 1 h, 2.) (1 mol prenyl bromide) 12 h 2: 80 percent / acetic anhydride / xylene / 11 h / 160 °C View Scheme
参考文献
Kaul, S. K.; Sehgal, C. K.; Taneja, S. C.; Dhar, K. L.; Atal, C. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 472 - 474
反应条件
tetrabutylammomium bromide; cadmium in tetrahydrofuran 6 h; Ambient temperature;
参考文献
Sain, Bir; Prajapati, Dipak; Sandhu, Jagir S.
Tetrahedron Letters, 1992 , vol. 33, # 33 p. 4795 - 4798
反应条件
tetrahydrofuran; Chromium (III) chloride; lithium aluminium tetrahydride in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Hiyama, Tamejiro; Okude, Yoshitaka; Kimura, Keizo; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 561 - 568
反应条件
1: 1.) NaH / diethyl ether 2: 41 percent / Wittig rearrangement View Scheme
参考文献
Bertrand, M.; Waegell, B.; Zahra, J. P.
Bulletin de la Societe Chimique de France, 1991 , # 6 p. 904 - 910
反应条件
acetic acid; zinc 1.) THF, 2.) irradiation; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Franck-Neumann, Michel; Martina, Daniel; Heitz, Marie-Paule
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6679 - 6682
反应条件
lithium diisopropyl amide 1) THF, -78 deg C, 30 min, 2) THF, 3 h; Multistep reaction;
参考文献
Kalena, Govind P.; Pradhan, Padmanava; Banerji, Asoke
Tetrahedron, 1999 , vol. 55, # 11 p. 3209 - 3218
