4-氰基-4-[[(十二烷硫基)硫酮甲基]硫基]戊酸合成路线 (共 2 条)
反应条件
in ethyl acetate
16 h; Heating / reflux;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/113493 A1, 2005 ;
Location in patent: Page/Page column 3; 4-5 ;
反应条件
1: sodium n-dodecyl trithiocarbonate With iodine in diethyl ether
1 h;
2: 4-cyanopentanoic acid in ethyl acetate
24 h; Reflux;
参考文献
Mitsubishi Rayon Co., Ltd.
Patent: US2012/309900 A1, 2012 ;
Location in patent: Page/Page column 14 ;