4,4,5,5-四甲基-2-[4-[(三甲基硅基)乙炔基]苯基]-1,3,2-二氧杂硼烷合成路线 （共 4 条）
反应条件
[{Ir(l-Cl)(CO)2}2]; N-ethyl-N,N-diisopropylamine in toluene T=80°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Kownacki, Ireneusz; Orwat, Bartosz; Marciniec, Bogdan; Kownacka, Agnieszka
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 548 - 550
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane T=-60°C;
参考文献
Newby, James A.; Huck, Lena; Blaylock, D. Wayne; Witt, Paul M.; Ley, Steven V.; Browne, Duncan L.
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 263 - 271
反应条件
boron trifluoride diethyl etherate in acetonitrile T=0 - 20°C; 1.5 h; Inert atmosphere;
参考文献
Zhu, Chuan; Yamane, Motoki
Organic Letters, 2012 , vol. 14, # 17 p. 4560 - 4563
反应条件
in diethyl ether T=20°C; 24 h;
参考文献
Iida, Hiroki; Shimoyama, Munenori; Furusho, Yoshio; Yashima, Eiji
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 417 - 423
