5-甲氧基-2-甲硫基-4-氯嘧啶合成路线 （共 4 条）
反应条件
N,N-dimethyl-aniline; trichlorophosphate Chlorination; 2 h; Heating;
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
反应条件
m-chloro-peroxy-benzoic acid in methanol; water; 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
VIFOR (INTERNATIONAL) AG
Patent: US2012/202806 A1, 2012 ;
反应条件
1: 98 percent / Zn; NH4Cl; H2O / benzene / 8 h / Heating 2: 87 percent / MCPBA / CH2Cl2 / 20 °C 3: 74 percent / NaOH; H2O / 50 °C View Scheme
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
反应条件
1: 98 percent / Zn; NH4Cl; H2O / benzene / 8 h / Heating
2: 87 percent / MCPBA / CH2Cl2 / 20 °C
View Scheme
参考文献
Jacobsen, Stig Andre; Rodbotten, Synne; Benneche, Tore
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 22 p. 3265 - 3268
