3-{[(2R)-3-甲氧基-3-氧代-2-(棕榈酰氨基)丙基]硫基}-1,2-丙烷二基二十六烷酸酯合成路线 （共 5 条）
反应条件
triethylamine in N,N-dimethyl-formamide
T=50°C; 30 h;
参考文献
Jung, Guenther; Carrera, Carlos; Brueckner, Hans; Bessler, Wolfgang G.
Liebigs Annalen der Chemie, 1983 , # 9 p. 1608 - 1622
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in tetrachloromethane
1 h; Ambient temperature;
参考文献
Jung, Guenther; Carrera, Carlos; Brueckner, Hans; Bessler, Wolfgang G.
Liebigs Annalen der Chemie, 1983 , # 9 p. 1608 - 1622
反应条件
1: 81 percent / triethylamine, 1,4-dithioerythritol / CHCl3 / 48 h
2: 80 percent / triethylamine / dimethylformamide / 20 h / 50 °C
3: 63 percent / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CCl4 / 1 h / Ambient temperature
View Scheme
参考文献
Jung, Guenther; Carrera, Carlos; Brueckner, Hans; Bessler, Wolfgang G.
Liebigs Annalen der Chemie, 1983 , # 9 p. 1608 - 1622
反应条件
1: 63 percent / N-methylmorpholine / CHCl3 / 2 h / Ambient temperature
2: 81 percent / triethylamine, 1,4-dithioerythritol / CHCl3 / 48 h
3: 80 percent / triethylamine / dimethylformamide / 20 h / 50 °C
4: 63 percent / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CCl4 / 1 h / Ambient temperature
View Scheme
参考文献
Jung, Guenther; Carrera, Carlos; Brueckner, Hans; Bessler, Wolfgang G.
Liebigs Annalen der Chemie, 1983 , # 9 p. 1608 - 1622
反应条件
1: 80 percent / triethylamine / dimethylformamide / 20 h / 50 °C
2: 63 percent / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CCl4 / 1 h / Ambient temperature
View Scheme
参考文献
Jung, Guenther; Carrera, Carlos; Brueckner, Hans; Bessler, Wolfgang G.
Liebigs Annalen der Chemie, 1983 , # 9 p. 1608 - 1622
