3-(三氟甲氧基)肉桂酸甲酯合成路线 (共 3 条)
反应条件
triethylamine in N,N-dimethyl-formamide; toluene
T=100°C; Heck Reaction; 20 h;
参考文献
Derible, Antoine; Becht, Jean-Michel; Le Drian, Claude
Tetrahedron Letters, 2013 , vol. 54, # 32 p. 4207 - 4209
反应条件
3-methoxy-2-hydroxybenzaldehydeiminato(thiosemicarbazone)(triphenylphosphane)palladium(II); sodium carbonate in N,N-dimethyl-formamide
T=140°C; Mizoroki-Heck reaction; 24 h; Inert atmosphere;
参考文献
Xie, Guanlei; Chellan, Prinessa; Mao, Jincheng; Chibale, Kelly; Smith, Gregory S.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1641 - 1647
反应条件
sulfuric acid
T=100°C; 5.5 h;
参考文献
Mitsubishi Tanabe Pharma Corporation
Patent: EP2168944 A1, 2010 ;
Location in patent: Page/Page column 175 ;