Palominos, Mario A.; Santos, Jose G.; Valderrama, Jaime A.; Vega, Juan C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2641 - 2643
in ethanol
T=0°C; 3 h; other periods of time; Product distribution;
参考文献
Palominos, Mario A.; Santos, Jose G.; Valderrama, Jaime A.; Vega, Juan C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2641 - 2643
in N,N-dimethyl-formamide
addn. of soln. of MCl2 in DMF to hot soln. of Schiff base in DMF (stirring), addn. of soln. of xanthate in water (stirring), pptn. on addn. of vater; filtration, washing (DMF), drying (over P4O10); elem. anal.;
参考文献
El-Said, Asma I.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 8 p. 1411 - 1426
in N,N-dimethyl-formamide
addn. of soln. of MCl2 in DMF to hot soln. of Schiff base in DMF (stirring), addn. of soln. of xanthate in water (stirring), pptn. on addn. of vater; filtration, washing (DMF), drying (over P4O10); elem. anal.;
参考文献
El-Said, Asma I.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 8 p. 1411 - 1426
