反-2-(3-甲氧苯基)乙烯基硼酸频哪醇酯合成路线 (共 2 条)
反应条件
triethylamine; Schwartz's reagent
T=60°C; 16 h;
参考文献
Wang, Yanong D.; Kimball, Gregory; Prashad, Amar S.; Wang, Yan
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8777 - 8780
反应条件
NaOC(CH3)3; CH3OH; [(N,N′-bis[2,6-diisopropylphenyl]imidazolin-2-ylidene)CuCl] in tetrahydrofuran
1.0 molpercent Cu-complex, alkyne, diborane, NaOC(CH3)3, CH3OH, THF, -15°C, 24 h, N2 atm.; 79:21 ratio of isomers;
参考文献
Jang, Hwanjong; Zhugralin, Adil R.; Lee, Yunmi; Hoveyda, Amir H.
Journal of the American Chemical Society, 2011 , vol. 133, # 20 p. 7859 - 7871