5,7-二甲基-2-苯基吡唑并[1,5-a]嘧啶合成路线 (共 13 条)
反应条件
1: 99 percent / 12 h / 100 °C 2: 13 percent / ethanol / 15 h / 100 °C View Scheme
参考文献
Danagulyan; Panosyan; Boyakhchyan
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 5 p. 581 - 585
参考文献
Nam; Grandberg; Sorokin
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 11 p. 1371 - 1374
反应条件
T=120°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
T=130°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
T=125°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
T=138°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
Tetrahedron, 2011 , vol. 67, # 12 p. 2279 - 2286
反应条件
hydrogenchloride in water
10 h; Reflux;
参考文献
Bassoude, Ibtissam; Berteina-Raboin, Sabine; Massip, Stephane; Leger, Jean-Michel; Jarry, Christian; Essassi, El Mokhtar; Guillaumet, Gerald
European Journal of Organic Chemistry, 2012 , # 13 p. 2572 - 2578
反应条件
in ethanol
5 h; Heating;
参考文献
Elmoghayer; Ibramin; El Sakka; et al.
Archiv der Pharmazie, 1983 , vol. 316, # 8 p. 697 - 702
反应条件
hydrogenchloride
1.5 h; Heating;
参考文献
Bellec, Christian; Lhommet, Gerard
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 6 p. 1793 - 1800
反应条件
in ethanol
T=100°C; 15 h;
参考文献
Danagulyan; Panosyan; Boyakhchyan
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 5 p. 581 - 585