1,1-双(三甲基甲硅烷基氧基)-3-甲基-1,3-丁二烯合成路线 （共 4 条）
反应条件
lithium diisopropyl amide
2 h; Ambient temperature;
参考文献
Brady, William T.; Agho, Michael O.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 501 - 506
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane
1.) -78 deg C to RT, 2.) RT, 1.5 h;
参考文献
Matsuda, Fuyuhiko; Kawasaki, Motoji; Ohsaki, Masako; Yamada, Kaoru; Terashima, Shiro
Tetrahedron, 1988 , vol. 44, # 18 p. 5745 - 5760
反应条件
1: 71 percent / hexamethyldisilazan/pyridine / tetrahydrofuran / 17 h / Ambient temperature
2: 74 percent / LDA / 2 h / Ambient temperature
View Scheme
参考文献
Brady, William T.; Agho, Michael O.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 501 - 506
反应条件
1.) -70 deg C, 12 h, 2.) from -70 deg C to RT; Yield given. Multistep reaction;
参考文献
Bellassoued, M.; Ennigrou, R.; Gaudemar, M.
Journal of Organometallic Chemistry, 1990 , vol. 393, # 1 p. 19 - 25
