1: With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: With tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-78 - 20°C;
3: With water in tetrahydrofuran; hexane
0.333333 h;
参考文献
Huang, Hsin-Hau; Prabhakar, Ch.; Tang, Kuo-Chun; Chou, Pi-Tai; Huang, Guan-Jhih; Yang, Jye-Shane
Journal of the American Chemical Society, 2011 , vol. 133, # 20 p. 8028 - 8039
1.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C
1.2: 90 percent / hexane; tetrahydrofuran / 0.5 h / 20 °C
2.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C
2.2: 78 percent / (iPrO)3B / hexane; tetrahydrofuran / 21 h / -78 - 20 °C
View Scheme
参考文献
Tavasli, Mustafa; Bettington, Sylvia; Bryce, Martin R.; Al Attar, Hameed A.; Dias, Fernando B.; King, Simon; Monkman, Andrew P.
Journal of Materials Chemistry, 2005 , vol. 15, # 46 p. 4963 - 4970
