triethylamine in toluene T=25°C; 15 h;

aluminum oxide T=250°C; P=2 - 5 Torr;

1: NaBO3*4H2O / acetic acid / 20 °C 2: methanesulfonyl chloride; triethylamine / CH2Cl2 / 20 °C View Scheme

1: K2CO3 2: NaBO3*4H2O / acetic acid / 20 °C 3: methanesulfonyl chloride; triethylamine / CH2Cl2 / 20 °C View Scheme

2-phthalimidoperacetic acid; N-hexadecyl-N,N,N-trimethylammonium bromide in water T=25°C; pH=7; 0.0833333 h; Product distribution; Further Variations:ReagentspH-values;

1: 83 percent / Na2CO3 / H2O / a) 70 deg C, 1 h, b) r.t., 13 h 2: 62 percent / 30percent H2O2, AcOH / 10 h / 23 °C 3: 89 percent / SOCl2, pyridine / CH2Cl2 / a) 0 deg C, 15 min, b) 40 deg C, 5 min 4: 97 percent / NEt3 / toluene / 15 h / 25 °C View Scheme

oxone in 1,4-dioxane; water T=25°C; pH 10; Rate constant;