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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87166-93-6
合成路线
（共 21 条）
35840-91-6
2-苄基吡咯烷
+
201230-82-2
→
反应条件
87166-93-6
反应条件
copper diacetate; air; palladium diacetate in toluene P=760 Torr; 24 h; Heating;
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Nakamura, Takatoshi; Horibata, Akiyoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Yamazaki, Tetsuro; Tokuda, Masao
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5951 - 5958
1069130-84-2
→
反应条件
87166-93-6
反应条件
1: With trifluoroacetic acid in dichloromethane T=0 - 20°C; Inert atmosphere; 2: With sodium carbonate in dichloromethane T=20°C; 3 h;
参考文献
Bertrand, Myra Beaudoin; Neukom, Joshua D.; Wolfe, John P.
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8851 - 8860
71739-76-9
→
反应条件
87166-93-6
反应条件
hydrogen; platinum(IV) oxide in acetic acid 16 h; Ambient temperature;
参考文献
Iwao, M.; Mahalanabis, K. K.; Watanabe, M.; Silva, S. O. De; Snieckus, V.
Tetrahedron, 1983 , vol. 39, # 12 p. 1955 - 1962
690256-02-1
→
反应条件
87166-93-6
+
83696-69-9
2-丙基-1(2H)-异喹啉酮
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 6 h; Heating;
参考文献
Osornio, Yazmin M.; Miranda, Luis D.; Cruz-Almanza, Raymundo; Muchowski, Joseph M.
Tetrahedron Letters, 2004 , vol. 45, # 13 p. 2855 - 2858
1245741-97-2
→
反应条件
87166-93-6
反应条件
sodium amalgam in methanol T=20°C; 4 h; Inert atmosphere;
参考文献
Brenzovich Jr., William E.; Benitez, Diego; Lackner, Aaron D.; Shunatona, Hunter P.; Tkatchouk, Ekaterina; Goddard III, William A.; Toste, F. Dean
Angewandte Chemie - International Edition, 2010 , vol. 49, # 32 p. 5519 - 5522
100-39-0
溴化苄
→
反应条件
87166-93-6
反应条件
1.1: sec-BuLi; TMEDA / diethyl ether; cyclohexane / 3.5 h / -78 °C 1.2: diethyl ether; cyclohexane / 20 °C 2.1: 0.56 g / CF3COOH / CH2Cl2 / 3 h / 20 °C 3.1: 83 percent / Cu(OAc)2; air / Pd(OAc)2 / toluene / 24 h / 760 Torr / Heating View Scheme
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Nakamura, Takatoshi; Horibata, Akiyoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Yamazaki, Tetsuro; Tokuda, Masao
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5951 - 5958
144688-81-3
→
反应条件
87166-93-6
反应条件
1: 0.56 g / CF3COOH / CH2Cl2 / 3 h / 20 °C 2: 83 percent / Cu(OAc)2; air / Pd(OAc)2 / toluene / 24 h / 760 Torr / Heating View Scheme
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Nakamura, Takatoshi; Horibata, Akiyoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Yamazaki, Tetsuro; Tokuda, Masao
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5951 - 5958
134612-93-4
→
反应条件
91639-72-4
+
87166-93-6
反应条件
2-methylpropane-2-thiol in benzene Irradiation;
参考文献
Newcomb, Martin; Esker, John L.
Tetrahedron Letters, 1991 , vol. 32, # 8 p. 1035 - 1038
91639-72-4
→
反应条件
87166-93-6
反应条件
1: COCl2, DMF / benzene; toluene / 12 h / Ambient temperature 2: diethyl ether 3: 13 percent / benzene / 10 h / Irradiation View Scheme
参考文献
Esker, John L.; Newcomb, Martin
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4933 - 4940
18159-24-5
→
反应条件
87166-93-6
反应条件
2: 86 percent / Zn-Cu couple, 10percent KOH / H2O; pyridine / 13 h / Heating 3: 100 percent / diethyl ether 4: 47 percent / hydrogen / PtO2 / acetic acid / 16 h / Ambient temperature View Scheme
参考文献
Iwao, M.; Mahalanabis, K. K.; Watanabe, M.; Silva, S. O. De; Snieckus, V.
Tetrahedron, 1983 , vol. 39, # 12 p. 1955 - 1962
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