乙酰基(3-乙酰基-7-甲氧基萘-1-基)氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
0.5 h;
参考文献
Scopton, Alex; Kelly, T. Ross
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 10004 - 10012
反应条件
1: NaH / dimethylformamide / 1.42 h / 0 - 20 °C
2: 5.41 g / CH2Cl2 / 1.08 h / 0 - 20 °C
3: 90 percent / AlCl3 / nitromethane; CH2Cl2 / 3 h / 0 - 20 °C
4: 95 percent / 4-(dimethylamino)pyridine / acetonitrile / 0.5 h
View Scheme
参考文献
Scopton, Alex; Kelly, T. Ross
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 10004 - 10012
反应条件
1: 90 percent / AlCl3 / nitromethane; CH2Cl2 / 3 h / 0 - 20 °C
2: 95 percent / 4-(dimethylamino)pyridine / acetonitrile / 0.5 h
View Scheme
参考文献
Scopton, Alex; Kelly, T. Ross
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 10004 - 10012
反应条件
1: 5.41 g / CH2Cl2 / 1.08 h / 0 - 20 °C
2: 90 percent / AlCl3 / nitromethane; CH2Cl2 / 3 h / 0 - 20 °C
3: 95 percent / 4-(dimethylamino)pyridine / acetonitrile / 0.5 h
View Scheme
参考文献
Scopton, Alex; Kelly, T. Ross
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 10004 - 10012
