in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature;

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in tetrahydrofuran addn. of 1 equiv. of phosphaketene to soln. of Pt-complex, stirring at room temp. for few hours; evapn., washing (petroleum ether), dissoln. (THF), layering (petroleum ether), crystn. on cooling to -25°C; NMR spectroscopy;