反应条件
1: With iPr2NBn; titanium tetrachloride in dichloromethane; 1,2-dichloro-ethane
T=0°C; Inert atmosphereReflux;
2: With methanol; ammonium chloride in dichloromethane; 1,2-dichloro-ethane
T=20°C; Inert atmosphereSaturated solution;
3: With hydrogenchloride; water in dichloromethane; 1,2-dichloro-ethane
参考文献
Crepin, Damien; Dawick, James; Aissa, Lhnstopne
Angewandte Chemie - International Edition, 2010 , vol. 49, # 3 p. 620 - 623
