(3-甲基噁丙环-2-基)甲醇合成路线 (共 9 条)
参考文献
Wang, Zhi; Cui, Yong-Tao; Xu, Zhao-Bing; Qu, Jin
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2270 - 2274
参考文献
National Distillers and Chemical Corporation
Patent: US4968817 A1, 1990 ;
反应条件
tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium in chlorobenzene
T=80°C; 5 h;
参考文献
Lempers; Ripolles i Garcia; Sheldon
Journal of Organic Chemistry, 1998 , vol. 63, # 5 p. 1408 - 1413
反应条件
tert.-butylhydroperoxide; titanium(IV) isopropylate in dichloromethane
1 h; Ambient temperature;
参考文献
Fraile, Jose M.; Garcia, Jose I.; Mayoral, Jose A.; Menorval, Louis C. de; Rachdi, Ferid
Journal of the Chemical Society, Chemical Communications, 1995 , # 5 p. 539 - 540
反应条件
dihydrogen peroxide; tetra-n-butyl-ammonium in acetonitrile
T=31.85°C; 14 h;
参考文献
Kamata, Keigo; Kotani, Miyuki; Yamaguchi, Kazuya; Hikichi, Shiro; Mizuno, Noritaka
Chemistry - A European Journal, 2007 , vol. 13, # 2 p. 639 - 648
反应条件
dihydrogen peroxide in benzonitrile
参考文献
Wang; Dumas; Wong
Tetrahedron Letters, 1993 , vol. 34, # 3 p. 403 - 406
反应条件
dihydrogen peroxide; titanium silicate
T=50°C; Epoxidation; Ring cleavage; Product distribution; Further Variations:various reaction time;
参考文献
Davies; McMorn; Bethell; Page; King; Hancock; Hutchings
Chemical Communications, 2000 , # 18 p. 1807 - 1808
反应条件
dihydrogen peroxide; titanium silicate
T=50°C; pH=4; Product distribution; Further Variations:CatalystspH-values;
参考文献
Davies, Lucinda J.; McMorn, Paul; Bethell, Donald; Bulman Page, Philip C.; King, Frank; Hancock, Frederick E.; Hutchings, Graham J.
Journal of Catalysis, 2001 , vol. 198, # 2 p. 319 - 327
反应条件
sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate
other reducing agent; Product distribution;
参考文献
Brown, Herbert C.; Lynch, Gary J.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 930 - 939