碘化1,2-二甲基吡啶鎓合成路线 （共 25 条）
反应条件
in butyraldehyde 12 h;
参考文献
CLARIANT INTERNATIONAL LTD.
Patent: EP1630205 A1, 2006 ;
Location in patent: Page/Page column 7 ;
反应条件
anschliessend Erhitzen mit wss. Natronlauge;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 24, p. 1868,1870
反应条件
1: t-BuOK / 1.) toluene, EtOH, 30 min. 2.) toluene, EtOH, 10 min 2: CH2Cl2 3: 66 percent / dimethylformamide / 98.4 h / 50 - 70 °C View Scheme
参考文献
Foye; Jones; Ghoshal; Almassian
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 57 - 62
反应条件
piperidine in methanol Heating;
参考文献
Matsui, Masaki; Kawamura, Shigeo; Shibata, Katsuyoshi; Muramatsu, Hiroshige
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 1 p. 71 - 74
反应条件
in water T=150°C; 30 h; other sulfites of cyclic amines; var. amine: amine bisulfite ratio; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 16, p. 830 - 833
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1071 - 1074
反应条件
piperidine; methanol
参考文献
Phillips
Journal of Organic Chemistry, 1947 , vol. 12, p. 333,334
反应条件
n-Pentyl nitrite; sodium ethanolate in ethanol 1.) 0-5 deg C, 2 h, 2.) reflux, 3 h;
参考文献
Katritzky, Alan R.; Patel, Ranjan C.; Shanta, Mohammed
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1888 - 1889
反应条件
in water T=150°C; 30 h; other sulfites of cyclic amines; var. amine: amine bisulfite ratio; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 16, p. 830 - 833
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1071 - 1074
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene Knoevenagel condensation; 0.5 h; Neat (no solvent)Grinding;
参考文献
Seiad, Linda Loucif; Villemin, Didier; Bar, Nathalie; Hachemi, Messaoud
Synthetic Communications, 2012 , vol. 42, # 5 p. 650 - 657
反应条件
in water T=150°C; 30 h; other sulfites of cyclic amines; var. amine: amine bisulfite ratio; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 16, p. 830 - 833
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1071 - 1074
