4-甲基-2,3-二氢噻吩 1,1-二氧化物合成路线 （共 10 条）
反应条件
water; palladium Hydrogenation;
参考文献
van Zuydewijn
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 445,455
反应条件
sodium hydride in N,N-dimethyl-formamide
2 h; Ambient temperature;
参考文献
Chou, Ta-shue; Tso, Hsi-Hua; Chang, Lee-Jean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 515 - 520
反应条件
sodium hydride in N,N-dimethyl-formamide
T=-4°C; 24 h;
参考文献
Chou, Ta-shue; Tso, Hsi-Hua; Chang, Lee-Jean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 515 - 520
反应条件
sodium hydride in N,N-dimethyl-formamide
T=25°C; 1 h;
参考文献
Polunin, E. V.; Kharchevnikov, A. P.; Kashin, A. N.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 5 p. 717 - 720
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 5 p. 775 - 778
反应条件
sodium hydride in N,N-dimethyl-formamide
T=-4°C; 24 h;
参考文献
Chou, Ta-shue; Tso, Hsi-Hua; Chang, Lee-Jean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 515 - 520
反应条件
dihydrogen peroxide; acetic acid
参考文献
Birch; McAllan
Journal of the Chemical Society, 1951 , p. 3411,3415
反应条件
1: sodium; liquid ammonia; methanol
2: acetic acid; aqueous (?) hydrogen peroxide
View Scheme
参考文献
Birch; McAllan
Journal of the Chemical Society, 1951 , p. 3411,3415
反应条件
1: Br2 / CHCl3 / 64 h / Heating
2: pyridine / acetone / 18 h / Ambient temperature
View Scheme
参考文献
Chou, Ta-shue; Chen, Mei-Man
Heterocycles, 1987 , vol. 26, # 11 p. 2829 - 2834
反应条件
nitric acid
Heating;
参考文献
Titova, M. V.; Berestovitskaya, V. M.; Perekalin, V. V.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1172 - 1173
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 6 p. 1322 - 1323
反应条件
in 1,4-dioxane; diethyl ether
参考文献
Mukhamedova,L.A. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 1182 - 1183
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 1426 - 1427
