5-(1,3-二氧戊环-2-基)-2-戊炔-1-醇合成路线 （共 4 条）
反应条件
2,4,6-trimethyl-pyridine; methanesulfonyl chloride; lithium chloride in N,N-dimethyl-formamide
1) 0 deg C, 20 min, 2) 4 h, RT;
参考文献
Deslongchamps, Pierre; Roy, Bernard L.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2068 - 2075
反应条件
2: 1.) HCl, 2.) NaBH4 / 1.) MeOH, H2O, 2.) MeOH
View Scheme
参考文献
Yamamoto, Makoto; Yoshitake, Makoto; Yamada, Kazutoshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 991 - 992
参考文献
Yamamoto, Makoto; Yoshitake, Makoto; Yamada, Kazutoshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 991 - 992
反应条件
2: 1.) HCl, 2.) NaBH4 / 1.) MeOH, H2O, 2.) MeOH
3: 73 percent / yellow HgO / dimethylformamide / 2 h / Heating
View Scheme
参考文献
Yamamoto, Makoto; Yoshitake, Makoto; Yamada, Kazutoshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 991 - 992
