5-甲氧基-3,3-二甲基-2-吲哚啉酮合成路线 (共 7 条)
反应条件
copper(I) oxide; 1,2-diamino-benzene; sodium t-butanolate in tert-butyl alcohol
T=100°C; 24 h; Sealed tube;
参考文献
Jhan, Yu-Huei; Kang, Ting-Wei; Hsieh, Jen-Chieh
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1155 - 1159
反应条件
copper(I) oxide; 1,2-diamino-benzene; sodium t-butanolate in tert-butyl alcohol
T=100°C; 24 h; Sealed tube;
参考文献
Jhan, Yu-Huei; Kang, Ting-Wei; Hsieh, Jen-Chieh
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1155 - 1159
反应条件
hydrogen; palladium on activated charcoal in methanol
P=2585.7 Torr; Ambient temperature;
参考文献
Lee; Huang; Lin; Shih
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 1 - 11
反应条件
copper(l) iodide; N-acetyl-glycine; potassium iodide; sodium hydroxide in tert-butyl alcohol
T=100°C; 24 h;
参考文献
Hsieh, Jen-Chieh; Cheng, An-Yi; Fu, Jun-Hao; Kang, Ting-Wei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 31 p. 6404 - 6409
反应条件
CaH2 in 1,2,3,4-tetrahydro-naphthalene
T=20 - 200°C; 2.5 h;
参考文献
Lee; Huang; Lin; Shih
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 1 - 11
反应条件
sodium hydroxide; aqueous HBr
参考文献
Sandoz Ltd.
Patent: US4622336 A1, 1986 ;
反应条件
LiAlH4; sulfuric acid in tetrahydrofuran; methanol hydrochloric acid
参考文献
Sandoz Ltd.
Patent: US4622336 A1, 1986 ;