(S)-1-(萘-2-基)丙烷-1-醇合成路线 （共 2 条）
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 20 °C
2: tri-cyclo-hexyl-phosphine; bis(1,5-cyclooctadiene)nickel (0) / toluene / 0.25 h / 70 °C / |Inert atmosphere; |Glovebox
View Scheme
参考文献
Yonova, Ivelina M.; Johnson, A. George; Osborne, Charlotte A.; Moore, Curtis E.; Morrissette, Naomi S.; Jarvo, Elizabeth R.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2422 - 2427
Angew. Chem., 2014 , vol. 126, # 9 p. 2454 - 2459,6
反应条件
1: dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C / |Inert atmosphere
2: NiCl2*glyme; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Wisniewska, Hanna M.; Swift, Elizabeth C.; Jarvo, Elizabeth R.
Journal of the American Chemical Society, 2013 , vol. 135, # 24 p. 9083 - 9090
